The Centro Nacional de Investigación sobre la Evolución Humana (CENIEH) has participated in a paper published in the journal Applied Clay Science, assessing the influence of the laboratory preparations in climatic and paleoclimatic studies that use isotopes. The results show that the preparation is an important process that, on certain occasions, could lead to modification of the initial isotopic ratios.

The CENIEH Geology and Archaeometry laboratories collaborated on the preparations and analyzed the mineralogy to understand the isotopic content of the authigenic clays used to investigate paleoenvironments. Authigenic clays are minerals commonly present in sediments and soils that are found in archaeopaleontological sites and other Quaternary media, and they can hold isotopes whose ratios offer information about the environmental conditions under which they formed.

Nevertheless, isolating the isotopes is a laborious process requiring numerous preparations and treatments, such as aqueous solutions and acid attacks, which can contaminate or alter the initial isotopic composition.

The authors analyzed the possible influence of the composition of the water used in these preparations when it comes to determining the isotopic composition of the hydrogen. To do this, they used samples from a geological survey carried out in the region of Afar (Ethiopia) and from the Sierra de Atapuerca sites (Gran Dolina, Burgos), diverse laboratory treatments, and two types of water with different hydrogen abundance.

This paper, led by Isidoro Campaña, a researcher at the Universidad de Málaga who completed his doctoral thesis on sedimentological identification and the cartography or karstic facies at the CENIEH Digital Mapping and 3D Analysis Laboratory, is the fruit of multidisciplinary work in which researchers and laboratories in the United States and France also participated.